发明名称 THEOBROMINE PRODUCTION PROCESS
摘要 <p>A process for preparing theobromine by methylating 3-methyl xanthine disodium salt comprises reacting 3-methyl xanthine disodium salt with dimethyl sulfate by using acetone as solvent in the presence of sodium carbonate and acidifying. The present application also provides a process for refining theobromine which comprises dissolving coarse theobromine in liquid alkaline solution, decolorizing, filtering, adding reducing agent in filtrate, and acidifying at 60-80 °C until pH is 5-6, filtering, and drying to obtain theobromine.</p>
申请公布号 WO2009089677(A1) 申请公布日期 2009.07.23
申请号 WO2008CN01998 申请日期 2008.12.12
申请人 PERRIGO TRADING (SHANGHAI) CO., LTD.;LI, XINGTAI;SHU, RUIYOU;FENG, YUSHENG;YANG, AIRONG;ZHAO, LI;BILMAN, NISSIM 发明人 LI, XINGTAI;SHU, RUIYOU;FENG, YUSHENG;YANG, AIRONG;ZHAO, LI;BILMAN, NISSIM
分类号 C07D473/04 主分类号 C07D473/04
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