| 摘要 |
Disclosed herein is a process for preparing a metal or nonmetal phthalocyanine by using both microwave and a milling device. Specifically, according to the process, anhydrous phthalic acid, phthalimide, 1,3-diiminoisoindoline, 1,2-dicyanobenzene, an halogen derivative thereof, an alkyl derivative thereof or an alkoxy derivative thereof is mixed with a metal chloride or an alkoxy metal and milled at 130ˆ¼250°C for 0.25ˆ¼15 hours by using microwave at a frequency of 0.1ˆ¼100GHz and a power of 100ˆ¼4,000W. Further disclosed is an apparatus for preparing a metal or nonmetal phthalocyanine. |
