发明名称 CRYSTAL POLYMORPH OF 2,2'-BIS(2-HYDROXYETHOXY)-1,1'-BINAPHTHALENE AND METHOD FOR PRODUCING SAME
摘要 Provided are a 2,2'-bis(2-hydroxyethoxy)-1,1'-binaphthalene crystal having a prescribed crystal form, and a method for producing 2,2'-bis(2-hydroxyethoxy)-1,1'-binaphthalene crystals, the method including: a step for precipitating first crystals of 2,2'-bis(2-hydroxyethoxy)-1,1'-binaphthalene from a first solution obtained by dissolving 2,2'-bis(2-hydroxyethoxy)-1,1'-binaphthalene in at least one type of solvent selected from aromatic hydrocarbons, and then obtaining a mother solution by solid-liquid separation; a step for preparing a second solution in which 2,2'-bis(2-hydroxyethoxy)-1,1'-binaphthalene is dissolved using at least part of the mother solution; and a step for precipitating second crystals of 2,2'-bis(2-hydroxyethoxy)-1,1'-binaphthalene from the second solution at a temperature of 60ºC or lower.
申请公布号 WO2015137238(A1) 申请公布日期 2015.09.17
申请号 WO2015JP56555 申请日期 2015.03.05
申请人 TAOKA CHEMICAL CO., LTD. 发明人 MATSUURA, TAKASHI;KAWAMURA, MIO;HIRABAYASHI, SHUNICHI;FUJII, KATSUHIRO
分类号 C07C43/23;C07C41/40 主分类号 C07C43/23
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