发明名称 PRODUCTION METHOD FOR POLYTHIOL COMPOUND POLYMERIZABLE COMPOSITION FOR OPTICAL MATERIAL AND USE THEREFOR
摘要 <p>This production method for a polythiol compound comprises: a step in which 2- mercaptoethanol and an epihalohydrin compound represented by general formula (1) are reacted at a temperature of 10- 50 °C in order to obtain a polyalcohol compound that is represented by formula (2); a step in which the obtained polyalcohol compound and thiourea are reacted in the presence of hydrogen chloride in order to obtain an isothiuronium salt; a step in which the temperature of a reaction solution containing the obtained isothiuronium salt is maintained at a temperature of 15- 60 °C and aqueous ammonia is added to said reaction solution within 80 minutes the isothiuronium salt is hydrolyzed, and a polythioi compound represented by formula (5) is obtained; and a step in which hydrochloric acid having a concentration of 25- 36% is added to a solution containing the obtained polythmol compound and washing is carried out at a temperature of 10- 50 °C in order to purify the polythiol compound.</p>
申请公布号 IN9747DEN2014(A) 申请公布日期 2015.07.31
申请号 IN2014DELNP9747 申请日期 2014.11.18
申请人 MITSUI CHEMICALS INC. 发明人 KAWAGUCHI MASARU;NISHIMURA TAKESHI
分类号 C07C319/20;C07C321/14;C08G18/38 主分类号 C07C319/20
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