发明名称 |
Method for producing inorganic oxide particles |
摘要 |
The present invention relates to a method for producing inorganic oxide particles, comprising at least the following steps of:
coagulating a dispersion obtained by carrying out the hydrolysis reaction and the polycondensation reaction of a metal alkoxide in the presence of a basic catalyst;
filtering the dispersion to obtain particles; anddrying the particles, whereinthe step of coagulating the dispersion is carried out by adding a coagulant comprising at least one compound selected from the group consisting of carbon dioxide, ammonium carbonate, ammonium hydrogen carbonate and ammonium carbamate to the dispersion.;The inorganic oxide particles obtained by the method of the present invention have high purity and are excellent in flowability. |
申请公布号 |
US9079777(B2) |
申请公布日期 |
2015.07.14 |
申请号 |
US201414533560 |
申请日期 |
2014.11.05 |
申请人 |
TOKUYAMA CORPORATION |
发明人 |
Maehara Takayuki;Komatsubara Tadaharu;Yamano Yuya;Ishizu Kenichi;Sato Makoto;Taira Hiroaki;Kato Hiroshi |
分类号 |
C07F7/02;C01B33/146;C01B13/36;C01B33/18;C01B33/148;C01G23/04;C01G25/02;C07F7/08;C07F7/10 |
主分类号 |
C07F7/02 |
代理机构 |
Birch, Stewart, Kolasch & Birch, LLP |
代理人 |
Birch, Stewart, Kolasch & Birch, LLP |
主权项 |
1. A method for producing inorganic oxide particles, comprising at least the following steps of:
coagulating a dispersion obtained by carrying out the hydrolysis reaction and the polycondensation reaction of a metal alkoxide in the presence of a basic catalyst by using of a mixture of water and an alcohol as a solvent; filtering the dispersion to obtain particles; and drying the particles, wherein the step of coagulating the dispersion is carried out by adding a coagulant comprising at least one compound selected from the group consisting of carbon dioxide, ammonium carbonate, ammonium hydrogen carbonate and ammonium carbamate to the dispersion. |
地址 |
Shunan-shi JP |