发明名称 Method for producing inorganic oxide particles
摘要 The present invention relates to a method for producing inorganic oxide particles, comprising at least the following steps of: coagulating a dispersion obtained by carrying out the hydrolysis reaction and the polycondensation reaction of a metal alkoxide in the presence of a basic catalyst; filtering the dispersion to obtain particles; anddrying the particles, whereinthe step of coagulating the dispersion is carried out by adding a coagulant comprising at least one compound selected from the group consisting of carbon dioxide, ammonium carbonate, ammonium hydrogen carbonate and ammonium carbamate to the dispersion.;The inorganic oxide particles obtained by the method of the present invention have high purity and are excellent in flowability.
申请公布号 US9079777(B2) 申请公布日期 2015.07.14
申请号 US201414533560 申请日期 2014.11.05
申请人 TOKUYAMA CORPORATION 发明人 Maehara Takayuki;Komatsubara Tadaharu;Yamano Yuya;Ishizu Kenichi;Sato Makoto;Taira Hiroaki;Kato Hiroshi
分类号 C07F7/02;C01B33/146;C01B13/36;C01B33/18;C01B33/148;C01G23/04;C01G25/02;C07F7/08;C07F7/10 主分类号 C07F7/02
代理机构 Birch, Stewart, Kolasch & Birch, LLP 代理人 Birch, Stewart, Kolasch & Birch, LLP
主权项 1. A method for producing inorganic oxide particles, comprising at least the following steps of: coagulating a dispersion obtained by carrying out the hydrolysis reaction and the polycondensation reaction of a metal alkoxide in the presence of a basic catalyst by using of a mixture of water and an alcohol as a solvent; filtering the dispersion to obtain particles; and drying the particles, wherein the step of coagulating the dispersion is carried out by adding a coagulant comprising at least one compound selected from the group consisting of carbon dioxide, ammonium carbonate, ammonium hydrogen carbonate and ammonium carbamate to the dispersion.
地址 Shunan-shi JP