发明名称 |
Method of graphene manufacturing |
摘要 |
A method for manufacturing graphene by vapor phase epitaxy on a substrate comprising a surface of SiC, characterized in that the process of sublimation of silicon from the substrate is controlled by a flow of an inert gas or a gas other than an inert gas through the epitaxial reactor. Graphene obtained by this method. |
申请公布号 |
US9067796(B2) |
申请公布日期 |
2015.06.30 |
申请号 |
US201113154920 |
申请日期 |
2011.06.07 |
申请人 |
INSTYTUT TECHNOLOGII MATERIALOW ELEKTRONICZNYCH |
发明人 |
Strupinski Wlodzimierz |
分类号 |
C01B31/04;B82Y30/00;B82Y40/00 |
主分类号 |
C01B31/04 |
代理机构 |
Westerman, Hattori, Daniels & Adrian, LLP |
代理人 |
Westerman, Hattori, Daniels & Adrian, LLP |
主权项 |
1. A method of manufacturing graphene in an epitaxial reactor, comprising
providing a substrate of SiC in the epitaxial reactor, introducing gaseous carbon precursor into the epitaxial reactor as an external carbon source, maintaining the SiC substrate at a temperature of above 1100° C. and depositing carbon on the SiC substrate by vapor phase epitaxial deposition, inhibiting or preventing sublimation of silicon from the SiC substrate by a flow of an inert gas or a gas other than an inert gas through the epitaxial reactor, wherein during said vapor phase epitaxial deposition the product of the inert gas or the gas other than the inert gas in the reactor and the inert gas or the gas other than the inert gas flow rate through the reactor is adjusted such that a stagnant layer of the inert gas or the gas other than the inert gas is created over the surface of said substrate, preventing silicon sublimation. |
地址 |
Warsaw PL |