发明名称 METHOD FOR PRODUCING COPPER (II) GLYCINATE (II) IN PRESENCE OF ACETOPHENONEOXIME
摘要 FIELD: chemistry.SUBSTANCE: invention refers to chemistry, more specifically to a method for producing copper glycinate that can find application as biologically active and feed additives. A method involves heating fine glycine powder and powdered copper in water (or dimethylformamide) at constant stirring of a reaction mixture. The precipitate is decanted, dissolved; the solution is filtered, boiled off partially; after cooling down with ethanol, copper (II) glycinate is deposited; the mixture is filtered; the complex is washed in petroleum ester and dried. Before heating, the reaction mixture is added with an oxidiser, which is presented by acetophenoneoxime in the following ratio, wt %: glycine - 3.35-6.00; copper - 1.52-2.60; water (or dimethylformamide) - 89.32-80.53; acetophenoneoxime - 5.81-10.87.EFFECT: method is implemented in the presence of acetophenoneoxime and enables increasing the copper (II) glycinate yield.1 ex
申请公布号 RU2553471(C2) 申请公布日期 2015.06.20
申请号 RU20130150769 申请日期 2013.11.14
申请人 FEDERAL'NOE GOSUDARSTVENNOE BJUDZHETNOE OBRAZOVATEL'NOE UCHREZHDENIE VYSSHEGO PROFESSIONAL'NOGO OBRAZOVANIJA "ASTRAKHANSKIJ GOSUDARSTVENNYJ TEKHNICHESKIJ UNIVERSITET" 发明人 OGORODNIKOVA NADEZHDA PETROVNA;KALAMBETOVA LJUBOV' SERGEEVNA;STARKOVA NATAL'JA NIKOLAEVNA;RJABUKHIN JURIJ IVANOVICH
分类号 C07C229/76;C07C227/18;C07F1/08 主分类号 C07C229/76
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