发明名称 Method for producing epoxy compound
摘要 To provide a method for producing an epoxy compound having fewer residual quaternary salt compound by removing the quaternary salt compound from an organic solution containing an epoxy compound and the quaternary salt compound.;A method for producing an epoxy compound comprising the following step 1, step 2, and step 3: step 1: a step in which in a mixture liquid containing an olefin compound, an aqueous hydrogen peroxide solution, a quaternary salt compound, a heteropoly acid, and an organic solvent, the olefin compound is subjected to the oxidation reaction to obtain an organic solution (A) containing an epoxy compound,step 2: a step in which an aqueous inorganic alkali solution is allowed to contact with the organic solution (A) to obtain an organic solution (B) containing the epoxy compound, andstep 3: a step in which an acidic aqueous solution containing a polymer having at least one functional group selected from the group consisting of a carboxyl group and a sulfonic acid group is allowed to contact with the organic solution (B) to obtain an organic solution (C) containing the epoxy compound.
申请公布号 US9045446(B2) 申请公布日期 2015.06.02
申请号 US201313934078 申请日期 2013.07.02
申请人 ARAKAWA CHEMICAL INDUSTRIES, LTD. 发明人 Sasagawa Naoki;Takumi Kiyoshi;Ezaki Yoichiro
分类号 C07D301/12 主分类号 C07D301/12
代理机构 Knobbe Martens Olson & Bear LLP 代理人 Knobbe Martens Olson & Bear LLP
主权项 1. A method for producing an epoxy compound comprising the following step 1, step 2, and step 3: step 1: a step in which in a mixture liquid containing an olefin compound, an aqueous hydrogen peroxide solution, a quaternary salt compound, a heteropoly acid, and an organic solvent, the olefin compound is subjected to the oxidation reaction to obtain an organic solution (A) containing an epoxy compound, step 2: a step in which an aqueous inorganic alkali solution is allowed to contact with the organic solution (A) to obtain an organic solution (B) containing the epoxy compound, and step 3: a step in which an acidic aqueous solution containing a polymer having at least one functional group selected from the group consisting of a carboxyl group and a sulfonic acid group is allowed to contact with the organic solution (B) to obtain an organic solution (C) containing the epoxy compound.
地址 Osaka-Shi JP