发明名称 |
Process for preparing lithium sulfide |
摘要 |
The invention relates to a novel process for preparing lithium sulfide and to the use thereof, wherein a reaction of lithium-containing strong bases with hydrogen sulfide is undertaken in an aprotic organic solvent within the temperature range from −20 to 120° C. under inert conditions. The lithium sulfide obtained by the process is used as a positive material in a galvanic element or for the synthesis of Li ion-conductive solids, especially for the synthesis of glasses, glass ceramics or crystalline products. |
申请公布号 |
US9017582(B2) |
申请公布日期 |
2015.04.28 |
申请号 |
US201214119980 |
申请日期 |
2012.05.29 |
申请人 |
Chemetall GmbH |
发明人 |
Rittmeyer Peter;Wietelmann Ulrich;Lischka Uwe;Hauk Dieter;Füger Bernhard;Stoll Armin;Dawidowski Dirk |
分类号 |
H01B1/06;C01B17/22;C01D15/00;H01M4/136;H01M4/58;H01M10/052 |
主分类号 |
H01B1/06 |
代理机构 |
Norton Rose Fulbright US LLP |
代理人 |
Norton Rose Fulbright US LLP |
主权项 |
1. A method for preparing lithium sulfide comprising:
reacting a lithium-containing base selected from the group consisting of a lithium alkylene, a lithium arylene, and a lithium amide with hydrogen sulfide in an aprotic organic solvent at a temperature of from −20° to 120° C. under inert conditions, wherein the aprotic organic solvent comprises at least one member selected from the group consisting of an aliphatic hydrocarbon, an aromatic hydrocarbon and an etheric solvent. |
地址 |
Frankfurt am Main DE |