发明名称 Liquid crystal polyester fibers and method for producing the same
摘要 Disclosed are liquid crystal polyester fibers, which have a peak half-width of 15° C. or greater at an endothermic peak (Tm1) observed by differential calorimetry under a temperature elevation of 20° C./minute from 50° C., polystyrene equivalent weight average molecular weight of 250,000 or more and 2,000,000 or less, and a variable waveform of less than 10% in terms of the half inert diagram mass waveform determined by a Uster yarn irregularity tester. Also disclosed is a method for producing liquid crystal polyester fibers, wherein liquid crystal polyester fibers are formed into a package, the fibers are then subjected to solid-phase polymerization, and the solid-phase polymerized liquid crystal polyester fibers are unrolled from the package and successively heat treated without being once taken up. The heat treatment temperature is controlled at a temperature of the endothermic peak temperature (Tm1) of the solid-phase polymerized liquid crystal polyester fibers+60° C. or higher, and the speeds of the fibers before and after heat treatment are regulated, respectively, by first and second rollers.
申请公布号 US9011743(B2) 申请公布日期 2015.04.21
申请号 US201013255524 申请日期 2010.03.04
申请人 Toray Industries, Inc. 发明人 Funatsu Yoshitsugu;Maeda Yuhei;Suzuki Norio;Katsuta Hiroo
分类号 D03D15/00;D06M15/643;C09K19/38;D01D10/02;D01F6/62;D01F6/84;D02J13/00 主分类号 D03D15/00
代理机构 Birch, Stewart, Kolasch & Birch, LLP 代理人 Birch, Stewart, Kolasch & Birch, LLP
主权项 1. A method for producing liquid crystal polyester fibers which comprises: forming liquid crystal polyester fibers into a package, subjecting said fibers to solid-phase polymerization, unrolling from said package solid-phase polymerized liquid crystal polyester fibers, and without further taking up into a package, successively heat treating said solid-phase polymerized liquid crystal polyester fibers, wherein the temperature of said heat treatment is controlled at a temperature of an endothermic peak temperature (Tm1) of said solid-phase polymerized liquid crystal polyester fibers+60° C. or higher, and a speed of said fibers before and after heat treatment is regulated, respectively, by a first roller and a second roller.
地址 Tokyo JP