发明名称 PRECIPITATION METHOD OF SPECIFIC CRYSTAL FORM BY SUBLIMATION/INVERSE-SUBLIMATION
摘要 <p>PROBLEM TO BE SOLVED: To provide a method for acquiring a specific crystal form efficiently and in a higher purity from a chemical compound having a crystal polymorphism.SOLUTION: Provided is a method for sublimating and introducing a chemical compound having two or more crystal polymorphisms into a collection part thereby to precipitate a specific crystal form by an inverse sublimation in the collection part, wherein the collection part is set at a temperature T satisfying the following formula (1): T2≤T≤T1, T1: a precipitation starting temperature by an inverse sublimation of said specific crystal form, and T2: a precipitation starting temperature by an inverse sublimation of a crystal form having a precipitation starting temperature lower than T1. However, there is no crystal form having a precipitation starting temperature between T1 and T2.</p>
申请公布号 JP2015067466(A) 申请公布日期 2015.04.13
申请号 JP20130201153 申请日期 2013.09.27
申请人 FUJIFILM CORP 发明人 SEO KIWAMU;ISHIDA SHINYA;NISHIDA YOICHI
分类号 C30B23/00;C07D219/02;C30B29/54 主分类号 C30B23/00
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