| 摘要 |
FIELD: chemistry.SUBSTANCE: invention relates to vacuum-plasma processing of composites. In processing of nanocomposites in hydrogen plasma applied is device which contains microwave oven, placed inside oven quartz reactor for placing in it of nanocomposites, consisting of case in form of hollow cylinder from quartz glass and installed on its ends with application of vacuum sealing from thermostable rubber dielectric flanges with shanks for connection with vacuum hoses, one of which is intended for supply of hydrogen into quartz reactor and is equipped with leak valve, and the other - for vacuuming microwave oven by means of mechanical pump. For processing nanocomposites are placed inside reactor, vacuuming of microwave oven and reactor is carried out by pumping out air with open leak valve after which hydrogen is supplied into reactor and washing of microwave oven and reactor with hydrogen is carried out, then leak valve is closed to obtain work pressure in reactor, after which, hydrogen plasma is inflamed in quartz reactor by SHF discharge and processing of nanocomposites with hydrogen is carried out.EFFECT: continuous processing of nanocomposites is provided.2 cl, 2 dwg |
