Real-time Automatic Analyzing method for Organic Pollutants of Fluid by using of Solid-Phase MicroExtraction-Gas Chromatograph(Gas Chromatograph/Mass Spectrometer Analyzing System

摘要

The present invention relates to a real-time automatic organic pollutant analysis method using a real-time SPME-GC or SPME-GC/MS analysis system in which an existing analyzer is used while a prompt response becomes possible based on prompt and accurate finding of the point in time when a high-concentration organic pollutant is generated through real-time and successive sampling. The present invention includes a sample supply step in which samples are successively supplied in real time to an accommodating portion of a sample bottle through a sample supply line formed in the real-time SPME-GC or SPME-GC/MS analysis system; and a sample analysis step for sample extraction and analysis using an analyzer (10) including a solid-phase micro extraction (SPME) for micro extraction of the sample of the real-time SPME-GC or SPME-GC/MS analysis system and a gas chromatograph/mass spectrometer for quantitative and qualitative analysis of the sample containing the organic pollutant after the supply of the sample extracted by the solid-phase micro extraction (SPME). According to the present invention, an existing analyzer can be used as it is while a follow-up measure becomes possible based on prompt and accurate finding of the point in time when the high-concentration organic pollutant is generated through real-time and successive sample supply. Also, no additional chemical is required for the sample analysis and sensitive analysis as well as chemical analysis can be facilitated.