发明名称 METHOD OF OBTAINING CIS-DICHLORODIAMMINEPLATINUM (II)
摘要 FIELD: chemistry.SUBSTANCE: invention relates to chemical industry. Compound of cis-dichlorodiammineplatinum (II) is obtained from solution of platinum coordination compound with further treatment with hydrochloric acid solution. As platinum coordination compound used is cis-dinitrodiammineplatinum (II), in which water is added. Obtained mixture is heated and mixture of urea and ethanol in ratio 1:1 is introduced, after which mixture is heated to 50-60°C. In alternative version solution of 17% sulphaminic acid is introduced at room temperature, with the following introduction of stoichiometric quantity of hydrochloric acid.EFFECT: invention makes it possible to increase target product purity to not less than 99,6% and its output to 88%.3 cl, 2 ex
申请公布号 RU2538895(C2) 申请公布日期 2015.01.10
申请号 RU20130107097 申请日期 2013.02.18
申请人 FEDERAL'NOE GOSUDARSTVENNOE BJUDZHETNOE UCHREZHDENIE NAUKI INSTITUT NEORGANICHESKOJ KHIMII IM. A.V.NIKOLAEVA SIBIRSKOGO OTDELENIJA ROSSIJSKOJ AKADEMII NAUK (INKH SO RAN) 发明人 GONCHAROVA EKATERINA SERGEEVNA;SHIPACHEV VLADIMIR ALEKSEEVICH;LEVCHENKO LJUDMILA MIKHAJLOVNA
分类号 C01G55/00 主分类号 C01G55/00
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