摘要 |
<p>Thus, according to the present invention there is provided a method for making a substantially pure higher MW phenylalkylsiloxane from a lower MW phenylalkylsiloxane by polymerisation of the lower MW phenylalkylsiloxane under vacuum in the presence of an aqueous alkaline solution containing one or more alkalis selected from the group of potassium hydroxide, magnesium hydroxide, calcium hydroxide, rhubidium hydroxide ammonium hydroxide, tetraalkylammonium hydroxide, tetraalkyl ammonium alkoxide and phosphonium hydroxides in an amount of from 50ppm or greater based upon the amount of lower MW phenylalkylsiloxane.</p> |