发明名称 PROCESS FOR THE MANUFACTURE OF EPOXY-MONOMERS AND EPOXIDES
摘要 A process for manufacturing epoxy monomers and/or epoxides in high yields and useful quality and chemical stability by dehydrochlorination of the corresponding chlorohydrins with an alkaline agent, producing the corresponding side product dry salt in a high purity, characterized in that the process comprises the following steps: a. Reaction of the chlorohydrins with the alkaline agent to form corresponding epoxides and the corresponding precipitated chloride salt; b. Dehydration, and optionally completing the reaction, of the reaction mixture of step (a), by use of an azeotropic agent, added to step (b) or generated in situ in step (a), resulting in the producing of a dehydrated reaction mixture; c. Separating the resulting chloride salt by filtration from the dehydrated reaction mixture (b) and d. Isolating the epoxide from the filtered liquid fraction.
申请公布号 WO2014198243(A1) 申请公布日期 2014.12.18
申请号 WO2014CZ00064 申请日期 2014.06.09
申请人 SPOLEK PRO CHEMICKOU A HUTNI VYROBU, AKCIOVA SPOLECNOST 发明人 KUBICEK, PAVEL;NEMECEK, BEDRICH;SLADEK, PETR
分类号 C07D301/26;C07D301/32 主分类号 C07D301/26
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