| 发明名称 |
METHOD OF COMBINED OBTAINING OF 1,2-EPOXYDODECANE AND 1,2-DODECANEDIOL |
| 摘要 |
FIELD: chemistry.SUBSTANCE: target product represents 1,2-epoxydodecane and combined with it 1,2-dodecanediol, in a weight ratio of 3:1. The catalytic oxidation of 1-dodecen with sodium hypochlorite is carried out with the application of the catalyst KBr for 10 h in the presence of a solvent - acetonitrile, with a volume ratio 1-dodecene:acetonitrile, equal to 1:8÷15.EFFECT: increased rate of carrying out the reaction and an increase of the target product output.3 dwg, 2 tbl, 5 ex |
| 申请公布号 |
RU2533420(C1) |
申请公布日期 |
2014.11.20 |
| 申请号 |
RU20130139763 |
申请日期 |
2013.08.27 |
| 申请人 |
FEDERAL'NOE GOSUDARSTVENNOE BJUDZHETNOE OBRAZOVATEL'NOE UCHREZHDENIE VYSSHEGO PROFESSIONAL'NOGO OBRAZOVANIJA "VOLGOGRADSKIJ GOSUDARSTVENNYJ TEKHNICHESKIJ UNIVERSITET" (VOLGGTU) |
发明人 |
ZOTOV JURIJ L'VOVICH;KRASIL'NIKOVA KLAVDIJA FEDOROVNA;POPOV JURIJ VASIL'EVICH;BUTAKOVA NATAL'JA ALEKSANDROVNA;BIRJUKOVA ALISA ALEKSEEVNA;BORSHCHEVA VIKTORIJA NIKOLAEVNA |
| 分类号 |
C07D301/12;C07C17/42;C07C27/16;C07C31/20 |
主分类号 |
C07D301/12 |
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