发明名称 Method for producing nanoparticles
摘要 A method for producing a nanoparticle to separate a diketopyrrolopyrrole pigment includes separating an α-type diketopyrrolopyrrole pigment nanoparticle having high crystallinity by carrying out separation of the diketopyrrolopyrrole pigment and crystal type transformation to the α-type with substantially a single step. The α-type diketopyrrolopyrrole pigment nanoparticle is separated by mixing a diketopyrrolopyrrole pigment solution having the diketopyrrolopyrrole pigment dissolved in a solvent and an alcohol solvent containing an alcohol compound solvent in a thin film fluid formed between at least two processing surfaces 1 and 2 arranged to be opposite to each other so as to be able to approach to and separate from each other, at least one of which rotates relative to the other. An acidic substance is contained in at least any one of the diketopyrrolopyrrole pigment solution and the alcohol solvent at this moment.
申请公布号 US8889885(B2) 申请公布日期 2014.11.18
申请号 US201113520239 申请日期 2011.02.01
申请人 M. Technique Co., Ltd. 发明人 Enomura Masakazu
分类号 B82Y40/00;C07D487/04;B01D9/00;C09B67/10;C09B67/48 主分类号 B82Y40/00
代理机构 Birch, Stewart, Kolasch & Birch, LLP 代理人 Birch, Stewart, Kolasch & Birch, LLP
主权项 1. A method for producing nanoparticles, the method comprising: providing at least two processing surfaces arranged opposite to each other, the at least two processing surfaces being configured to be able to approach to and separate from each other, at least one of which rotating relative to the other; providing at least two kinds of fluids to be processed, wherein, at least one of the at least two kinds of fluids is a diketopyrrolopyrrole pigment solution containing at least one kind of diketopyrrolopyrrole pigment dissolved in a solvent and at least one of the at least two kinds of fluids other than the above-mentioned is an alcohol solvent containing at least one kind of alcohol compound solvent; and mixing the at least two kinds of fluids to be processed to separate the diketopyrrolopyrrole pigment thereby providing the method for producing the nanoparticles, wherein: of the diketopyrrolopyrrole pigment solution and the alcohol solvent, at least any one of the fluids to be processed contains an acidic substance, the diketopyrrolopyrrole pigment solution and the alcohol solvent are mixed in a thin film fluid formed between the at least two processing surfaces, thereby separating the diketopyrrolopyrrole pigment, and a pH value of a mixed solution obtained by mixing the at least two kinds of fluids in the thin film fluid formed between the at least two processing surfaces is less than or equal to 7, so that substantially only α-type diketopyrrolopyrrole pigment nanoparticles are separated without substantially separating a β-type diketopyrrolopyrrole pigment.
地址 Osaka JP