发明名称 METHOD FOR OBTAINING HIERARCHICALLY ORDERED INORGANIC PHOSPHATE STRUCTURES ON PHYLLOSILICATES
摘要 The present invention relates to a method for preparing hierarchically ordered structures of inorganic phosphate particles, homogeneously deposited on the surface of a phyllosilicate, which is characterized in that it comprises the following steps: a) obtaining an acid solution of precursor compounds of an inorganic phosphate; b) preparing a dispersion of particles of a phyllosilicate in aqueous medium and acidifying the phyllosilicate dispersion by adding at least one acid, thereby obtaining an acid dispersion; c) mixing the acid solution obtained in step a) with the dispersion obtained in step b); and d), with stirring, adding a base to the mixture obtained in step c) until the required pH value for precipitating the corresponding inorganic phosphate on the phyllosilicate particles has been achieved, resulting in a hierarchically ordered structure of homogeneously distributed submicrometric or nanometric inorganic phosphate particles supported on the phyllosilicate surface.
申请公布号 US2014336318(A1) 申请公布日期 2014.11.13
申请号 US201214366145 申请日期 2012.05.14
申请人 Esteban Cubillo Antonio;Santaren Rome Julio;Aguilar Diez Eduardo;Alvarez Berenguer Antonio;Palacios Zambrano Elena;Leret Molto Maria Pilar;Fernandez Lozano Jose Francisco;De aza Moya Antonio Heliodoro;Rodriguez Barbero Miguel Angel 发明人 Esteban Cubillo Antonio;Santaren Rome Julio;Aguilar Diez Eduardo;Alvarez Berenguer Antonio;Palacios Zambrano Elena;Leret Molto Maria Pilar;Fernandez Lozano Jose Francisco;De aza Moya Antonio Heliodoro;Rodriguez Barbero Miguel Angel
分类号 C09K21/12;C09C1/28;C08K5/5415;C08K3/32;C09K21/04;C08K3/34 主分类号 C09K21/12
代理机构 代理人
主权项 1. A method for preparing hierarchically ordered structures of inorganic phosphate particles, homogenously deposited on the surface of a phyllosilicate, wherein it comprises the following steps: a) obtaining an acid solution of precursor compounds of an inorganic phosphate, b) preparing a dispersion of particles of a phyllosilicate in aqueous medium and acidifying the phyllosilicate dispersion by adding at least one acid, thereby obtaining an acid dispersion, c) mixing the acid solution obtained in step a) with the dispersion obtained in step b) d) with stirring, adding a base to the mixture obtained in step c) until the pH value required for precipitating the corresponding inorganic phosphate on the phyllosilicate particles is achieved, resulting in a hierarchically ordered structure of homogenously distributed submicrometric or nanometric inorganic phosphate particles, supported on the phyllosilicate surface.
地址 Madrid ES