发明名称 |
Tensometer for simultaneously evaluating polymerization stresses, shrinkage and modulus development |
摘要 |
The present invention relates to apparatus and method for evaluating the development of PS during polymerization of dental restorative composites, which includes using a tensometer for measuring deflection of a calibrated cantilever beam induced by PS and calculating PS from the measured deflection. A tensometer according to an embodiment of the present invention can be used to quantify PS at varying beam locations and heights, and determine trend in PS development as a function of beam length. More importantly, in the present invention, the development of polymerization shrinkage and the elastic modulus can be simultaneously obtained in real time. |
申请公布号 |
US8857266(B2) |
申请公布日期 |
2014.10.14 |
申请号 |
US201113282600 |
申请日期 |
2011.10.27 |
申请人 |
The United States of America, as Represented by the Secretary of Commerce, The National Institute of Standards and Technology |
发明人 |
Chiang Martin |
分类号 |
G01N3/08;G01N3/20 |
主分类号 |
G01N3/08 |
代理机构 |
Rankin, Hill & Clark LLP |
代理人 |
Bandy Mark E.;Rankin, Hill & Clark LLP |
主权项 |
1. A method for determining the development of polymeric shrinkage during polymer material curing, the method comprising:
curing a first sample of the polymeric material having a predetermined length, wherein the first sample of the polymeric material is coupled to a cantilever beam at first predetermined position; measuring deflection of the cantilever beat at predetermined time intervals until the polymeric material curing is complete; coupling a second sample of the polymeric material having the predetermined length to the cantilever beam at a second predetermined position; curing the second sample of the polymeric material; measuring deflection of the cantilever beam at the predetermined time intervals until the second sample of the polymeric material curing is complete; and determining linear shrinkage and elastic modulus of the polymeric material at the predetermined time intervals. |
地址 |
Gaithersburg MD US |