发明名称 |
HOLLOW SILLICA SPHERES SYNTHETIC METHOD USING OF SURFACTANT |
摘要 |
The present invention relates to a method for synthesizing a hollow nano-silica material using a surfactant, comprising: (a) a step of adding hydrochloric acid (HCl) in an aqueous ethanol solution; (b) a step of adding a surfactant to the HCl-added solution and making the solution react at room temperature; (c) a step of adding tetraethylorthosilcate (TEOS) to the solution and making the solution react at room temperature; (d) a step of adding ammonia water to the solution; (e) a step of obtaining precipitate followed by washing and drying the precipitate; and (f) a step of plasticizing the dried precipitate. The present invention uses critical micelle concentration of the surfactant to easily adjust the surfactant in a core producing process, and the surfactant can be easily removed at relatively low temperatures when removed, thereby easily producing a hollow nano-silica material with a simple process. In addition, the micelle structure used in the present invention can be adjustable into a molecular size of the surfactant, thereby adjusting the size of a core material 100 nm or less. |
申请公布号 |
KR20140115629(A) |
申请公布日期 |
2014.10.01 |
申请号 |
KR20130030418 |
申请日期 |
2013.03.21 |
申请人 |
INDUSTRY ACADEMIC COOPERATION FOUNDATION KEIMYUNGUNIVERSITY |
发明人 |
BAE, JAE YOUNG;YUN, TAE KWAN;LEE, JONG TAK |
分类号 |
C01B33/12;B01J6/00 |
主分类号 |
C01B33/12 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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