发明名称 Methods for producing a thin film consisting of nanosheet monolayer film(s) by spin coat methods, and hyperhydrophilized materials, substrates for an oxide thin film and dielectric materials obtained therefrom
摘要 To provide a method for producing a thin film consisting of nanosheet monolayer film(s) and use of the thin film obtained thereby.;The method for producing a thin film consisting of nanosheet monolayer film(s) by a spin coat method according to the invention comprises a step for preparing an organic solvent sol formed by allowing nanosheets obtained by the exfoliation of an inorganic layered compound to be dispersed in an organic solvent; and a step for dropping the organic solvent sol onto a substrate and rotating the substrate using a spin coater. Preferably, the nanosheet size, the organic solvent sol concentration and the spin coater rotation speed are controlled.
申请公布号 US8828488(B2) 申请公布日期 2014.09.09
申请号 US201213591372 申请日期 2012.08.22
申请人 National Institute For Materials Science 发明人 Sasaki Takayoshi;Saruwatari Kazuko;Matsuba Kazuaki;Akatsuka Kousyo;Ebina Yasuo;Osada Minoru
分类号 B05D3/12;B05D3/06;B32B5/16;B82Y30/00;B82Y40/00 主分类号 B05D3/12
代理机构 Wenderoth, Lind & Ponack, L.L.P. 代理人 Wenderoth, Lind & Ponack, L.L.P.
主权项 1. A method for producing a thin film consisting of nanosheet monolayer film(s) in which nanosheets obtained by the exfoliation of an inorganic layered compound are aligned densely without overlapping in every monolayer by a spin coat method comprising: a step for preparing an organic solvent sol formed by allowing nanosheets to be dispersed in an organic solvent; and a step for dropping the organic solvent sol onto a substrate and rotating the substrate using a spin coater; wherein the inorganic layered compound is selected from the group consisting of layered perovskite oxide, layered manganese oxide, layered cobalt oxide, layered manganese-cobalt oxide, layered manganese-iron oxide, layered tungsten oxide, layered niobium oxide, layered tantalum oxide, layered titanium-niobium oxide, layered titanium-tantalum oxide, layered molybdenum oxide, and layered ruthenium oxide, in the step involving rotating, the relationship between the organic solvent sol concentration and the spin coater rotation speed is a relationship of a quadratic function, and the relationship of a quadratic function depends on the type and the size of the nanosheet.
地址 Ibaraki JP