发明名称 METHOD OF SYNTHESISING 1,6-HEXAMETHYLENEDIAMINE- N, N'-DISUCCINIC ACID
摘要 FIELD: chemistry.SUBSTANCE: method includes preparation of reaction solution by dissolving maleic anhydride in water, addition of solutions of alkaline reagent, representing lithium hydroxide, and 1,6-hexanediamine, boiling solution, bringing solution pH to 2.6 by means of concentrated solution of hydrobromic acid, product crystallisation, separation of crystals from solution, and purification of product from inorganic substances - by-products of reactions that take place on solution. Purification of final product from lithium bromide is carried out in one stage by means of hot acetone.EFFECT: method makes it possible to obtain product of higher purity without loss of output.1 tbl, 1 ex
申请公布号 RU2527271(C1) 申请公布日期 2014.08.27
申请号 RU20130106188 申请日期 2013.02.14
申请人 FEDERAL'NOE GOSUDARSTVENNOE BJUDZHETNOE OBRAZOVATEL'NOE UCHREZHDENIE VYSSHEGO PROFESSIONAL'NOGO OBRAZOVANIJA "TVERSKOJ GOSUDARSTVENNYJ UNIVERSITET" 发明人 JAKOVLEV ALEKSEJ ALEKSEEVICH;NIKOL'SKIJ VIKTOR MIKHAJLOVICH;TOLKACHEVA LJUDMILA NIKOLAEVNA;SIMONOVA MARIJA VLADIMIROVNA
分类号 C07C229/16;C07C227/22 主分类号 C07C229/16
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