发明名称 SULFUR-CONTAINING PALLADIUM/CARBON CATALYST, PREPARATION METHOD THEREFOR, AND METHOD FOR PREPARING P-PHENYLENEDIAMINE ANTIOXIDANT
摘要 <p>Provided are a sulfur-containing Palladium (Pd)/carbon catalyst, a preparation method therefor, and a method of using the catalyst to prepare p-Phenylenediamine (PPD) rubber antioxidant. The method for preparing the sulfur-containing Pd/carbon catalyst comprises: loading Pd on an active carbon to obtain a Pd/carbon catalyst; then, preparing a slurry by mixing the Pd/carbon catalyst with a solvent; subsequently, adding a sulfide to the slurry, stirring at a predetermined temperature; finally, filtering, and acquiring the sulfur-containing Pd/carbon catalyst. Application of the sulfur-containing Pd/carbon catalyst in the preparation of the PPD rubber antioxidant not only improves the yield of the PPD rubber antioxidant and inhibits a material from being reduced into a corresponding alcohol, but also improves selectivity.</p>
申请公布号 EP2759341(A1) 申请公布日期 2014.07.30
申请号 EP20120834431 申请日期 2012.09.24
申请人 JIANGSU SINORGCHEM TECHNOLOGY CO., LTD. 发明人 LI, XIAONIAN;ZHANG, QUNFENG;CHEN, XINMIN;FENG, FENG;MA, LEI;LU, CHUNSHAN;LI, CHUNSHENG
分类号 B01J31/16;B01J37/20;C07C209/26;C07C211/51 主分类号 B01J31/16
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