Radial mixing devices for rotating inclined reactors

摘要

Disclosed in this specification is the design for an internal mixing device which increases the plug flow like behavior of the rotating inclined reactor.

主权项

1. Use of an inclined cylindrical rotating reactor comprising an axis of rotation, granules of polyester treated within the reactor, a granules of polyester flow regime, at least two mixing devices and an inert purge gas, for the solid state polymerization of the granules of polyester, wherein the granules of material treated within the reactor comprise a polyester and the reactor has a temperature in the range of about 140° C. to about 235° C.
the axis of rotation is central and not parallel to the horizontal line perpendicular to the force of gravity, the granules of polyester flow regime is characterized by a Froude Number Fr=(ω2×R/g)
comprised in the range of 1×10−4 to 0.5;where ω is the angular velocity of the reactor;R is the internal radius of the reactor and g is the gravity of acceleration=9.806 m/s; and each of the at least two mixing devices has a height, width, and an equivalent length defined as the distance between the plane perpendicular to the axis of rotation that contains the point where the mixing device first protrudes from the reactor wall and the plane perpendicular to the axis of rotation that contains the point where the mixing device stops protruding from the wall and the equivalent length of the mixing device is selected from the group consisting of equivalent lengths less than 1/10th the length of the reactor, so as the granules of the polyester treated within the reactor pass through the reactor due to the force of gravity as well as the reactor rotation with a plug flow like behavior; and the at least two mixing devices are connected in a manner so that the inert purge gas can pass from the first mixing device to the second mixing device through a connector; said use comprising the steps of:
introducing the granules into the top of the reactorpassing the granules through the reactor while subjecting the granules to a stream of inert purge gas below the turbulent rate.