摘要 |
The invention relates to a method for recycling of phosphoric acid solution from a decontamination bath, which solution is contaminated with radioactive components, wherein the used phosphoric acid solution is diluted with aqueous oxalic acid solution, in order to separate off iron oxalate in this connection, and the phosphoric acid solution is used for decontamination of further system parts, wherein the iron ion content in the phosphoric acid in the decontamination bath is continuously measured, and phosphoric acid is continuously withdrawn from the decontamination bath and concentrated and purified phosphoric acid is replaced, so that a specific concentration of dissolved iron in the contamination bath is not exceeded, and to a system for implementation of the method. The solution has the advantage that only small amounts of phosphoric acid are in circulation in a system for recycling of a phosphoric acid solution from a decontamination bath, whereby the required work volume in the system tanks is significantly reduced. Resulting from this, it is possible to undertake purging of iron ions stemming from electrochemical decontamination, from phosphoric acid solution, using mobile systems. |
主权项 |
1. Method for recycling of phosphoric acid solution from a decontamination bath (4), which solution is contaminated with radioactive components, wherein the used phosphoric acid solution is diluted with aqueous oxalic acid solution, in order to separate off iron oxalate in this connection, and the phosphoric acid solution is used for decontamination of further system parts, wherein
the iron ion content in the phosphoric acid (3b) in the decontamination bath (4) is continuously measured, phosphoric acid (3b) is continuously withdrawn from the decontamination bath (4) and concentrated and purified phosphoric acid (3a) is replaced, so that a specific concentration of dissolved iron in the contamination bath (4) is not exceeded. |