发明名称 METHOD OF STABILIZING ALPH-SIALON PHOSPHOR RAW POWDER, ALPH-SIALON PHOSPHOR COMPOSITION OBTAINED THEREFROM, AND METHOD OF MANUFACTURING ALPHA-SIALON PHOSPHOR
摘要 Disclosed herein is a method of stabilizing alpha-sialon phosphor raw powder, including the steps of: mixing alpha-sialon phosphor raw powder including Si3N4, AlN, a rare-earth metal oxide and calcium nitride (Ca3N2) as a calcium source and having Composition Formula represented by CaxSi12−m−nAlm+nOnN16−n:Rey (here, Re is an activator and is at least one selected from the group consisting of Eu, Ce, Tb, Yb, Sm and Dy, 0.3≦m≦1.0, 0.02≦y≦0.15, m=2x+3y); and heat-treating the alpha-sialon phosphor raw powder to convert the calcium source into a Ca—Al—Si—N based compound. This method is advantageous in that a reliable alpha-sialon phosphor having high photoluminescence intensity can be manufactured regardless of weather, season, environment and the like.
申请公布号 US2014191159(A1) 申请公布日期 2014.07.10
申请号 US201313761110 申请日期 2013.02.06
申请人 MACHINERY & MATERIALS KOREA INSTITUTE OF 发明人 KIM Jin Myung;LEE Jae Wook;PARK Young Jo
分类号 C09K11/77 主分类号 C09K11/77
代理机构 代理人
主权项 1. A method of stabilizing alpha-sialon phosphor raw powder, comprising the steps of: mixing alpha-sialon phosphor raw powder including Si3N4, AlN, a rare-earth metal oxide and calcium nitride (Ca3N2) as a calcium source and having Composition Formula represented by CaxSi12−m−nAlm+nOnN16−n:Rey (here, Re is an activator and is at least one selected from the group consisting of Eu, Ce, Tb, Yb, Sm and Dy, 0.3≦m≦1.0, 0.02≦y≦0.15, m=2x+3y); and heat-treating the alpha-sialon phosphor raw powder to convert the calcium source into a Ca—Al—Si—N based compound.
地址 US