发明名称 |
1,3-diiodohydantoin compound and production method thereof |
摘要 |
The present invention provides a means which can inhibit release of I2 in production or storage of 1,3-diiodohydantoin compound, and thereby solve decrease in purity of the compound and various problems caused by I2. The present invention provides a production method for 1,3-diiodohydantoin compound comprising a step to prepare a wet body containing a 1,3-diiodohydantoin compound, and (1) a step to dry the wet body by contacting the wet body with heated gas or (2) a step to lyophilize the wet body, a storage method for 1,3-diiodohydantoin compound comprising a step to store a 1,3-diiodohydantoin compound under a temperature condition of 15° C. or lower, and a 1,3-diiodohydantoin compound wherein content of released I2 is 1% by mass or less. |
申请公布号 |
US8772506(B2) |
申请公布日期 |
2014.07.08 |
申请号 |
US201012926900 |
申请日期 |
2010.12.16 |
申请人 |
Nippoh Chemicals Co., Ltd. |
发明人 |
Inoue Kazuhisa;Hanamura Yukihiko;Miyazawa Takaaki |
分类号 |
C07D233/82 |
主分类号 |
C07D233/82 |
代理机构 |
Buchanan Ingersoll & Rooney P.C. |
代理人 |
Buchanan Ingersoll & Rooney P.C. |
主权项 |
1. A production method for 1,3-diiodohydantoin compound, comprising:
a step to prepare a composition comprising a 1,3-diiodohydantoin compound, and a step to dry the composition by contacting the composition with a heated gas to inhibit release of I2 from the 1,3-diiodohydantoin compound so that a content of released I2 of the 1,3-diiodohydantoin compound is 1% by mass or less and a content of water of the 1,3-diiodohydantoin compound is 6% by mass or less, wherein the composition is contacted by flowing with the heated gas, and wherein a flow rate of the heated gas in contact with the composition is 0.1 to 10.0 m/sec. |
地址 |
Tokyo JP |