发明名称 1,3-diiodohydantoin compound and production method thereof
摘要 The present invention provides a means which can inhibit release of I2 in production or storage of 1,3-diiodohydantoin compound, and thereby solve decrease in purity of the compound and various problems caused by I2. The present invention provides a production method for 1,3-diiodohydantoin compound comprising a step to prepare a wet body containing a 1,3-diiodohydantoin compound, and (1) a step to dry the wet body by contacting the wet body with heated gas or (2) a step to lyophilize the wet body, a storage method for 1,3-diiodohydantoin compound comprising a step to store a 1,3-diiodohydantoin compound under a temperature condition of 15° C. or lower, and a 1,3-diiodohydantoin compound wherein content of released I2 is 1% by mass or less.
申请公布号 US8772506(B2) 申请公布日期 2014.07.08
申请号 US201012926900 申请日期 2010.12.16
申请人 Nippoh Chemicals Co., Ltd. 发明人 Inoue Kazuhisa;Hanamura Yukihiko;Miyazawa Takaaki
分类号 C07D233/82 主分类号 C07D233/82
代理机构 Buchanan Ingersoll & Rooney P.C. 代理人 Buchanan Ingersoll & Rooney P.C.
主权项 1. A production method for 1,3-diiodohydantoin compound, comprising: a step to prepare a composition comprising a 1,3-diiodohydantoin compound, and a step to dry the composition by contacting the composition with a heated gas to inhibit release of I2 from the 1,3-diiodohydantoin compound so that a content of released I2 of the 1,3-diiodohydantoin compound is 1% by mass or less and a content of water of the 1,3-diiodohydantoin compound is 6% by mass or less, wherein the composition is contacted by flowing with the heated gas, and wherein a flow rate of the heated gas in contact with the composition is 0.1 to 10.0 m/sec.
地址 Tokyo JP