| 发明名称 |
Process for preparing 1,1,2-Trichloro-3,3,3-trifluoropropane |
| 摘要 |
Disclosed is a process for making the compound 1,1,2-trichloro-3,3,3-trifluoropropane (233da) by the catalytic fluorination of 1,1,1,2,3,3-hexachloropropane. 233da is a starting material used in the production cis-1-chloro-3,3,3-trifluoropropene (cis-1233zd). |
| 申请公布号 |
US8754273(B2) |
申请公布日期 |
2014.06.17 |
| 申请号 |
US201213674160 |
申请日期 |
2012.11.12 |
| 申请人 |
Honeywell International Inc. |
发明人 |
Zhai Yian;Poss Andrew Joseph;Singh Rajiv Ratna |
| 分类号 |
C07C17/20;C07C19/01;C07C19/10;C07C17/04 |
主分类号 |
C07C17/20 |
| 代理机构 |
|
代理人 |
Wilson Erika S. |
| 主权项 |
1. A process for making the compound 1,1,2-trichloro-3,3,3-trifluoropropane (233da) from 1,1,1,2,3,3-hexachloropropane comprising the steps:
(a) fluorinating a metal catalyst consisting of SbCl5; and (b) fluorinating 1,1,1,2,3,3-hexachloropropane in the presence of the fluorinated metal catalyst at a reaction temperature in the range of 90° C. to 100° C. for a time period in the range of 6 to 20 hours, to produce a reaction mixture containing up to about 35% by weight of 1,1,2-trichloro-3,3,3-trifluoropropane.
|
| 地址 |
Morristown NJ US |
