发明名称 PROCESS FOR PRODUCTION OF SODIUM BOROHYDRIDE and diphenyl oxide
摘要 A process for production of an alkali metal borohydride. The process comprises three steps. The first step is combining a phenyl ester of a boric acid ester precursor with a compound of formula MAlH4-31 x(OPh)x, where x is from zero to three, M is an alkali metal and Ph is phenyl; to produce an alkali metal borohydride and Al(OPh)3. The second step is separating sodium borohydride from Al(OPh)3. The third step is heating Al(OPh)3 to produce diphenyl oxide.
申请公布号 US2014161703(A1) 申请公布日期 2014.06.12
申请号 US201214232627 申请日期 2012.07.18
申请人 Elowe Paul R.;Molzahn David C. 发明人 Elowe Paul R.;Molzahn David C.
分类号 C01B6/21 主分类号 C01B6/21
代理机构 代理人
主权项 1. A process for production of an alkali metal borohydride; said process comprising steps of: (a) combining a phenyl ester of a boric acid ester precursor with a compound of formula MAlH4−x(OPh)x, where x is from zero to three, M is an alkali metal and Ph is phenyl; to produce an alkali metal borohydride and Al(OPh)3; (b) separating sodium borohydride from Al(OPh)3; and (c) heating Al(OPh)3 to produce diphenyl oxide.
地址 Midland MI US