发明名称 |
Process for manufacturing bis(2-methoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracene |
摘要 |
A process to manufacture substituted tetracyano-hexaazatricyclics with the substitutions occurring at the 9 and 10 hydrogens. The process begins with 2,3-dichloro-5,6-dicyanopyrazine, which is reacted to form the desired tetracyano-hexaazatricyclic. Different process embodiments enable different reaction paths to the desired tetracyano-hexaazatricyclic. Different tetracyano-hexaazatricyclic embodiments include bis(2-methoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracene and bis(2-methoxyethoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracene. |
申请公布号 |
US8742107(B1) |
申请公布日期 |
2014.06.03 |
申请号 |
US201213691842 |
申请日期 |
2012.12.02 |
申请人 |
Vinazene, Inc. |
发明人 |
Rasmussen Paul George;Lawton Richard Graham |
分类号 |
C07D487/14 |
主分类号 |
C07D487/14 |
代理机构 |
|
代理人 |
|
主权项 |
1. A process for manufacturing bis(2-methoxyethyl)-2,3,6,7-tetracyano-1,4,5,8,9,10-hexazaanthracene, the process comprising:
refluxing 5,6-dicyano-2-(2-methoxyethyl)amino-3-chloropyrazine in a mixture of diethylene glycol dimethyl ether and N,N-diisopropyl-N-ethylamine.
|
地址 |
Ann Arbor MI US |