发明名称 METHOD FOR PRODUCING N,N-DIALKYLHOMOFARNESIC ACID AMIDE
摘要 PROBLEM TO BE SOLVED: To provide a method for producing an N,N-dialkylhomofarnesic acid amide which is a precursor of (±)-3a,6,6,9a-tetramethyldodecahydronaphtho[2,1-b]furan useful as a fragrance with a high raw material recovery rate, high purity and high yield and a method for producing (±)-3a,6,6,9a-tetramethyldodecahydronaphtho[2,1-b]furan.SOLUTION: There is provided a method for producing an N,N-dialkylhomofarnesic acid amide by reacting nerolidol with N,N-dialkylformamide dimethyl acetal under conditions where the N,N-dialkylformamide dimethyl acetal is refluxed, wherein the molar ratio of the N,N-dialkylformamide dimethyl acetal to nerolidol is 1.5 to 3.
申请公布号 JP2014097970(A) 申请公布日期 2014.05.29
申请号 JP20130209087 申请日期 2013.10.04
申请人 KAO CORP 发明人 YANO KENJI;AOKI TAKASHI
分类号 C07C231/10;C07C233/09;C07D307/92 主分类号 C07C231/10
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