发明名称 PROCESS FOR PRODUCTION OF (METH)ACRYLIC ACID
摘要 The objective of the present invention is to provide a process for producing highly pure (meth)acrylic acid stably and efficiently with crystallization. The process for production of (meth)acrylic acid according to the present invention is characterized in comprising the steps of cooling a crude (meth)acrylic acid solution in a crystallization apparatus until the temperature of a cooling medium discharged from the crystallization apparatus is stabilized in the range of higher than the solidification point of the crude (meth)acrylic acid solution in the crystallization apparatus and not more than the solidification point plus 5°C; then bringing the crude (meth)acrylic acid solution in the crystallization apparatus to a supercooled condition by setting the temperature of a cooling medium supplied to the crystallization apparatus at the temperature of not more than the solidification point of the crude (meth)acrylic acid solution minus 1°C; and crystallizing (meth)acrylic acid from the crude (meth)acrylic acid solution.
申请公布号 EP2433924(A4) 申请公布日期 2014.05.14
申请号 EP20100777668 申请日期 2010.05.07
申请人 NIPPON SHOKUBAI CO., LTD. 发明人 ISHII, YOSHITAKE;UENO, KOJI
分类号 C07C51/43;B01D9/00;C07C57/07 主分类号 C07C51/43
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