发明名称 Production of self-supporting ceramic materials having a reduced thickness and containing metal oxides
摘要 The present invention relates to a method for manufacturing a metal-oxide-based ceramic, including, in order, the step of inserting, into a flash sintering device, a nanocrystalline powder comprising crystallites and crystallite agglomerates of a ceramic of formula, Zr1-xMxO2, where M is chosen from yttrium, scandium and cerium, or Ce1-xM'xO2, where M' is chosen from gadolinium, scandium, samarium and yttrium, where x lies between 0 and 0.2, the powder having an average crystallite size of between 5 and 50 nm, an average crystallite agglomerate size of between 0.5 and 20 mum, and a specific surface area of between 20 and 100 m2/g. The invention further includes the step of flash sintering the powder by applying a pressure of between 50 and 150 MPa, at a temperature of between 850° C. and 1400° C., for a time of between 5 and 30 minutes.
申请公布号 US8652703(B2) 申请公布日期 2014.02.18
申请号 US201013377880 申请日期 2010.06.16
申请人 ZAHID MOHSINE;RIEU MATHILDE;ESTOURNES CLAUDE;LENORMAND PASCAL;ANSART FLORENCE;ELECTRICITE DE FRANCE;UNIVERSITE PAUL SABATIER TOULOUSE III 发明人 ZAHID MOHSINE;RIEU MATHILDE;ESTOURNES CLAUDE;LENORMAND PASCAL;ANSART FLORENCE
分类号 H01M8/10 主分类号 H01M8/10
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