| 发明名称 |
METHOD OF PRODUCING PALLADIUM BETA-KETOIMINATES |
| 摘要 |
FIELD: chemistry.SUBSTANCE: invention relates to a method of producing palladium (II) beta-ketoiminates. The method involves reacting palladium dichloride with a beta-ketoiminate. The palladium dichloride in aqueous solution of concentrated ammonia (NH(concentrated):HO - 25:25 ml) is transferred into an ampoule which is then placed in a microwave oven reactor and excess beta-ketoimine (in ratio of 1:(2-3)) dissolved in ethanol is then added. The mixture is exposed to 100-150 W microwaves to heat the solution for 2-30 minutes at temperature of 90-110°C. The end product is separated by filtration and the residue is dried on air.EFFECT: simple method, shorter duration of the method, high output of end products.2 cl, 3 ex |
| 申请公布号 |
RU2506268(C1) |
申请公布日期 |
2014.02.10 |
| 申请号 |
RU20120140632 |
申请日期 |
2012.09.21 |
| 申请人 |
FEDERAL'NOE GOSUDARSTVENNOE BJUDZHETNOE OBRAZOVATEL'NOE UCHREZHDENIE VYSSHEGO PROFESSIONAL'NOGO OBRAZOVANIJA "NOVOSIBIRSKIJ NATSIONAL'NYJ ISSLEDOVATEL'SKIJ GOSUDARSTVENNYJ UNIVERSITET" (NOVOSIBIRSKIJGOSUDARSTVENNYJ UNIVERSITET, NGU) |
发明人 |
ZHERIKOVA KSENIJA VASIL'EVNA;MIKHEEV ALEKSANDR NIKOLAEVICH;ZHARKOVA GALINA IVANOVNA;MOROZOVA NATAL'JA BORISOVNA;IGUMENOV IGOR' KONSTANTINOVICH;ARZHANNIKOV ANDREJ VASIL'EVICH;TUMM MANFRED KASPAR ANDREAS |
| 分类号 |
C07F15/00 |
主分类号 |
C07F15/00 |
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