发明名称 |
PURIFING METHODE FOR IONIC LIQUID EMI-BF_4 |
摘要 |
The present invention relates to a purifying method for high purity ionic liquid 1-ethyl-3-methylimidazolium tetrafluoroborate (EMI-BF4) comprising: a step of preparing synthesized EMI-BF4 (1-ethyl-3-methylimidazolium tetrafluoroborate); a step of removing precipitates existing in the synthesized EMI-BF4 by passing the synthesized EMI-BF4 through a glass filter; a step of performing primary vacuum distillation on the EMI-BF4 in which precipitates are removed; a step of mixing a distilled water mixture and the EMI-BF4 in a predetermined ratio and extracting ionic liquids with a liquid/liquid continuous extraction process by an extraction solvent; a step of drying the extracted ionic liquid by removing moisture; and a step of performing secondary vacuum distillation on the dried EMI-BF4. [Reference numerals] (AA) Filtration; (BB) Vacuum distillation (100mmHg↓24hr, 10mmHg↓24hr); (CC) Mixing with a distilled water in a predetermined ratio; (DD) Extracting for 48 hours by an extraction solvent (dichloromethane); (EE) Drying (MgSO_4 anhydrous) vacuum distillation (100mmHg↓24hr, 1mmHg↓48hr); (FF) High purity ionic liquid (Purified 1-ethyl-3-methylimidazolium tetrafluoroborate) |
申请公布号 |
KR20140013802(A) |
申请公布日期 |
2014.02.05 |
申请号 |
KR20120082351 |
申请日期 |
2012.07.27 |
申请人 |
CAPSOLUTION CO., LTD. |
发明人 |
LEE, YOUNG HWAN;CHUN, KUNG SOO;YANG, KYUNG CHUL;KIM, HYUNG CHAN;JEONG, GYWONG SIG;LEE, KWANG JE |
分类号 |
C07F5/02;B01D3/14;C07D233/12 |
主分类号 |
C07F5/02 |
代理机构 |
|
代理人 |
|
主权项 |
|
地址 |
|