发明名称 PROCESS FOR PRODUCING COPPER PHTHALOCYANINE COMPOUND
摘要 PROBLEM TO BE SOLVED: To provide a process for producing a copper phthalocyanine compound capable of preventing blockage of a gas discharge pipe during an imidation reaction by a simple reform of a production apparatus.SOLUTION: The process for producing a copper phthalocyanine compound comprises: (a) allowing phthalic acid and ammonia to react with each other in an organic solvent to obtain phthalimide, discharging gas containing at least the organic solvent and steam as a reaction product from a reaction apparatus, and allowing the reaction to proceed while liquefying the discharged organic solvent gas in the discharge pipe and returning the solvent to the reaction apparatus, as a first step; and (b) allowing the phthalimide obtained in the first step to react with a copper compound and urea in the presence of a catalyst to obtain a copper phthalocyanine compound, as a second step. In the first step, a temperature (T1) of the discharge pipe is set to a temperature satisfying the relation of T2&le;T1<T3 with respect to the boiling point (T2) and the boiling point (T3) of the organic solvent under the pressure in the first step.
申请公布号 JP2014005210(A) 申请公布日期 2014.01.16
申请号 JP20120139839 申请日期 2012.06.21
申请人 DIC CORP 发明人 TAKAHASHI MASAYOSHI;TAYAMA SADAZUMI;ONO KOJI
分类号 C07D487/22;C07B61/00;C07F1/08;C09B47/06 主分类号 C07D487/22
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