发明名称 PROCESS FOR PRODUCING CATALYST METAL LAYER AND PROCESS FOR PRODUCING GRAPHENE MATERIAL
摘要 <p>First, a quadrilateral substrate (12) comprising c-plane sapphire is prepared, and nickel is deposited as a catalyst metal on the entire upper surface of the substrate (12) to form a catalyst metal film (14) (see (a)). Next, the catalyst metal film (14) is patterned by lithography to form a catalyst metal film (16) having a given shape (see (b)). Subsequently, the temperature of the catalyst metal film (16) is elevated to 1,000ºC and kept at 1,000ºC for 20 minutes. The temperature of the catalyst metal film (16) is then lowered from 1,000ºC to 800ºC at a rate of 5 ºC/min and is kept at 800ºC for 15 hours. Thus, a catalyst metal layer (17) constituted of large grains is obtained (see (c)). Thereafter, a carbon source is supplied to the surface of the catalyst metal layer (17) to grow graphene, and the catalyst metal layer (17) is dissolved away with an acidic solution to take out a graphene material (10) (see (d) to (g)).</p>
申请公布号 WO2013129312(A1) 申请公布日期 2013.09.06
申请号 WO2013JP54762 申请日期 2013.02.25
申请人 MEIJO UNIVERSITY 发明人 NARITSUKA, SHIGEYA;MARUYAMA, TAKAHIRO
分类号 B01J23/755;B01J35/02;B01J37/08;C01B31/02 主分类号 B01J23/755
代理机构 代理人
主权项
地址