发明名称 |
Process for preparing 1,2-benzoisothiazoline-3-one |
摘要 |
Sodium sulfide hydrate is at least partially dehydrated by heating with N-methyl 2-pyrrolidone. 2-chlorobenzamide is added to the mixture which is heated further. The mixture is cooled and treated with aqueous hydrogen peroxide to give the sodium salt of 1,2-benzoisothiazoline-3-one in good yield. Acidification if desired gives rise to the free 1,2-benzoisothiazoline-3-one.
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申请公布号 |
US8476452(B2) |
申请公布日期 |
2013.07.02 |
申请号 |
US201113281600 |
申请日期 |
2011.10.26 |
申请人 |
BERG CARSTEN;SINGH SANGITA;TITAN CHEMICALS LIMITED |
发明人 |
BERG CARSTEN;SINGH SANGITA |
分类号 |
C07D275/04 |
主分类号 |
C07D275/04 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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