发明名称 |
PROCESS FOR PREPARING A SOL-GEL FROM AT LEAST THREE METAL SALTS AND USE OF THE PROCESS FOR PREPARING A CERAMIC MEMBRANE |
摘要 |
Process for preparing a sol-gel from at least four salts of metals M1, M2, M3 and M4 suitable and intended for the preparation of a perovskite type material corresponding to the general formula (I): A(1-X) A'x B(1-y-U) B'y B"u Omicron3-delta, (I), said process comprising the following steps: - a step a) of preparing an aqueous solution of water-soluble salts of said elements A, A' optionally A", B and B', in the stoichiometric proportions necessary for obtaining the material as defined above; - a step b) of preparing an aqueous-alcoholic solution of at least one non-ionic surfactant in an alcohol chosen from methanol, ethanol, propanol, propanol, isopropanol or butanol, mixed with an aqueous solution of ammonia in a sufficient proportion to ensure the complete solubilisation of said non-ionic surfactant in said aqueous-alcoholic solution, the concentration of said non-ionic surfactant in said aqueous-alcoholic solution being less than the critical micelle concentration; - a step c) of mixing said aqueous solution prepared in step a) with said alcoholic dispersion prepared in step b) in order to form a sol; - a step d) of drying said sol obtained in step c), by evaporation of the solvent, in order to obtain a sol-gel. Use of the process for preparing a ceramic membrane. |
申请公布号 |
WO2013087241(A1) |
申请公布日期 |
2013.06.20 |
申请号 |
WO2012EP68923 |
申请日期 |
2012.09.26 |
申请人 |
L'AIR LIQUIDE,SOCIETE ANONYME POUR L'ETUDE ET L'EXPLOITATION DES PROCEDES GEORGES CLAUDE;CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE;UNIVERSITE DE LIMOGES;RICHET, NICOLAS;CHARTIER, THIERRY;ROSSIGNOL, FABRICE;VIVET, AURELIEN;GEFFROY, PIERRE-MARIE |
发明人 |
RICHET, NICOLAS;CHARTIER, THIERRY;ROSSIGNOL, FABRICE;VIVET, AURELIEN;GEFFROY, PIERRE-MARIE |
分类号 |
C04B35/01;C01G15/00;C01G23/00;C01G49/00;C01G51/04;C04B35/26;C04B35/465;C04B38/06;C04B41/00;H01M4/86;H01M4/88;H01M4/90 |
主分类号 |
C04B35/01 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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