发明名称 Benzocarbazole-intercalated layered double hydroxides composite luminescent material and its preparation method
摘要 The present invention discloses a benzocarbazole-intercalated layered double hydroxides (LDHs) composite luminescent material and its preparation method. The detailed procedure comprises preparing divalent and trivalent metal cation solution A and glycol solution B of sodium 2-hydroxy benzo[a]carbazole-3-carboxylate, mixing the solutions A and B to obtain solution C, slowly adding the prepared NaOH solution dropwise into the solution C, regulating pH of the resultant after dropwise addition to obtain slurry D, allowing the slurry D to react under water bath or microwave temperature-controlled heating condition, centrifuging and washing the obtained product, and drying in vacuum to obtain 2-hydroxy benzo[a]carbazole-3-carboxylate anion intercalated LDHs composite material. The method implements the immobilization of sodium 2-hydroxy benzo[a]carbazole-3-carboxylate, effectively improves thermal stability of the luminescent dye molecules, and reduces fluorescence quenching caused by aggregation of the dye molecules.
申请公布号 US8309741(B2) 申请公布日期 2012.11.13
申请号 US20090459793 申请日期 2009.07.07
申请人 YAN DONGPENG;LU JUN;WEI MIN;DUAN XUE;BEIJING UNIVERSITY OF CHEMICAL TECHNOLOGY 发明人 YAN DONGPENG;LU JUN;WEI MIN;DUAN XUE
分类号 C07F5/06;C07D209/82 主分类号 C07F5/06
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