发明名称 |
Method for spinning and washing aramid fiber and recovering sulfuric acid |
摘要 |
A method for spinning and washing aramid fiber and for recovering sulfuric acid by (a) spinning an aramid polymer from a sulfuric acid spin dope to a yarn and coagulating the yarn in a coagulation bath having an inlet for water or diluted sulfuric acid and an outlet for sulfuric acid enriched water; (b) washing the yarn with water to obtain a washed yarn and a washing water containing sulfuric acid; (c) recycling the sulfuric acid enriched water and optionally the washing water to a sulfuric acid recovery unit; (d) increasing the sulfuric acid content of the recycled sulfuric acid enriched water, and optionally the washing water, by evaporation to obtain 20 to 98% sulfuric acid and water; (e) mixing the 20 to 98% sulfuric acid with oleum to obtain 98-105% sulfuric acid; and (f) recycling the 98-105% sulfuric acid to the spinning unit for use as sulfuric acid spin dope. |
申请公布号 |
US8273134(B2) |
申请公布日期 |
2012.09.25 |
申请号 |
US20080739643 |
申请日期 |
2008.10.10 |
申请人 |
KALSBEEK ESTHER CHRISTINA;BRUINING WESSEL JOSEPH;TEIJIN ARAMID B.V. |
发明人 |
KALSBEEK ESTHER CHRISTINA;BRUINING WESSEL JOSEPH |
分类号 |
D01H7/00;D01F9/30 |
主分类号 |
D01H7/00 |
代理机构 |
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代理人 |
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主权项 |
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地址 |
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