发明名称 METHOD OF PRODUCING (ACETYLACETONATO-2-O,O')(BIS-ACETONITRILE)PALLADIUM TETRAFLUOROBORATE
摘要 FIELD: chemistry. ^ SUBSTANCE: present invention relates to a method of producing (acetylacetonato-k2-O,O')(bis-acetonitrile)palladium tetrafluoroborate (where acac denotes acetyl acetonate, MeCN denotes acetonitrile). The method involves reaction of bis(acetylacetonato)palladium Pd(acac)2 with acetonitrile and a boron compound in the medium of an organic solvent at room temperature. The boron compound used is boron trifluoride etherate BF3OEt2, the organic solvent used is aromatic solvents, specifically benzene or toluene. ^ EFFECT: invention increases output of (acetylacetonato-k2-O,O')(bis-acetonitrile)palladium tetrafluoroborate. ^ 2 ex
申请公布号 RU2456295(C1) 申请公布日期 2012.07.20
申请号 RU20110112364 申请日期 2011.03.31
申请人 GOSUDARSTVENNOE OBRAZOVATEL'NOE UCHREZHDENIE VYSSHEGO PROFESSIONAL'NOGO OBRAZOVANIJA IRKUTSKIJ GOSUDARSTVENNYJ UNIVERSITET 发明人 SUSLOV DMITRIJ SERGEEVICH;TKACH VITALIJ SERGEEVICH;BYKOV MIKHAIL VALER'EVICH;BELOVA MARINA VLADIMIROVNA
分类号 C07F5/02;C07F15/00 主分类号 C07F5/02
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