发明名称 Processes for production of 2-bromo-2,2-difluoroethanol and 2-(alkylcarbonyloxy)-1, 1-difluoroethanesulfonic acid salt
摘要 Disclosed is a process for producing 2-bromo-2,2-difluoroethanol, which comprises reducing a bromodifluoroacetic acid derivative represented by the formula [1] by using an ate hydride complex as a reducing agent. 2-Bromo-2,2-difluoroethanol thus produced can be used as the starting material to carry out the esterification step, the sulfination step and the oxidation step in this order, thereby producing a 2-alkylcarbonyloxy-1,1-difluoroethanesulfonic acid salt, wherein A represents a substituted or unsubstituted linear, branched or cyclic alkoxy group having 1 to 20 carbon atoms, a substituted or unsubstituted aryloxy group having 6 to 15 carbon atoms, a heteroaryloxy group having 4 to 15 carbon atoms, or a halogen atom.
申请公布号 US8222448(B2) 申请公布日期 2012.07.17
申请号 US201113223605 申请日期 2011.09.01
申请人 JODRY JONATHAN JOACHIM;NAGAMORI MASASHI;HAGIWARA YUJI;FUJIWARA MASAKI;NARIZUKA SATORU;CENTRAL GLASS COMPANY, LIMITED 发明人 JODRY JONATHAN JOACHIM;NAGAMORI MASASHI;HAGIWARA YUJI;FUJIWARA MASAKI;NARIZUKA SATORU
分类号 C07C69/54 主分类号 C07C69/54
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