发明名称 Method for continuously producing oxidized cyclic phenol sulfides
摘要 The present invention discloses a method for continuously producing an oxidized cyclic phenol sulfide which comprises the continuous steps of reacting a para-alkyl phenol compound as a raw material with 1.7 to 2.5 molar equivalent of sulfur and 0.25 to 0.75 molar equivalent of an alkali metal reagent per 1 mol of the phenol compound (the first step); and oxidizing a cyclic phenol sulfide of the formula (2) produced by the above reaction with an oxidizing agent(s) in the same reactor as that of the first step and without taking the cyclic phenol sulfide out of the reactor: wherein R represents a straight or branched alkyl group having 1 to 6 carbon atoms, and m is an integer from 4 to 8, to obtain an oxidized cyclic phenol sulfide of the formula (3) (the second step): wherein R represents a straight or branched alkyl group having 1 to 6 carbon atoms, m is an integer from 4 to 8, and n is 1 or 2.
申请公布号 US8222428(B2) 申请公布日期 2012.07.17
申请号 US20090867207 申请日期 2009.02.16
申请人 YASUMURA MASATERU;AOKI YOSHIKAZU;ITO MASAMI;HODOGAYA CHEMICAL CO., LTD. 发明人 YASUMURA MASATERU;AOKI YOSHIKAZU;ITO MASAMI
分类号 C07D341/00 主分类号 C07D341/00
代理机构 代理人
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