| 摘要 |
A sample holder comprises a first thermal mass, a second thermal mass, and a sample vessel, the first and second thermal masses being movable relative to each other thereby to selectively place one or other in thermal contact with the sample vessel, at least one of the thermal masses being held at an elevated temperature. By moving the thermal masses appropriately, the sample holder can be brought into contact with each selectively, adjusting its temperature toward that of the thermal mass with which it is in contact relatively rapidly to allow close and rapid control of the sample temperature. The sample vessel is preferably biased toward the second thermal mass and can be slidably supported on at least one pin extending from the second thermal mass. The first thermal mass and/or the second thermal mass can comprise at least one block of copper. The second thermal mass can comprise, a pair of copper blocks/located either side of the first thermal mass. Generally, we prefer that it is the first thermal mass that is held at an elevated temperature. This allows the sample to default to a cool(er) state. |
