发明名称 METHOD OF PRODUCING POTASSIUM ACETATE
摘要 FIELD: chemistry. ^ SUBSTANCE: invention relates to a method of producing potassium acetate by reacting potassium hydroxide with aqueous acetic acid solution and subsequent steps for treating the obtained potassium acetate. The method involves filtration treatment of the obtained potassium acetate solution, evaporation of the filtrate at 105-115C, cooling to 55-65C and vacuum crystallisation. The method is characterised by that the starting products used are crystalline potassium hydroxide and 40-60% acetic acid, which is added to potassium hydroxide in 30-35% stoichiometric excess and while keeping temperature of the reaction mass at 80-90C, and that the potassium acetate crystals formed after the vacuum crystallisation step are further centrifuged at 500-2000 rpm and then vacuum dried at 145-155C. ^ EFFECT: method enables to obtain a highly pure product with minimal content of heavy metal impurities. ^ 1 cl, 2 tbl, 11 ex
申请公布号 RU2455279(C1) 申请公布日期 2012.07.10
申请号 RU20110119304 申请日期 2011.05.16
申请人 ROSSIJSKAJA FEDERATSIJA, OT IMENI KOTOROJ VYSTUPAET MINISTERSTVO OBRAZOVANIJA I NAUKI ROSSIJSKOJ FEDERATSII;FEDERAL'NOE GOSUDARSTVENNOE UNITARNOE PREDPRIJATIE "GOSUDARSTVENNYJ ORDENA TRUDOVOGO KRASNOGO ZNAMENI NAUCHNO-ISSLEDOVATEL'SKIJ INSTITUT KHIMICHESKIKH REAKTIVOV I OSOBO CHISTYKH KHIMICHESKIKH VESHCHESTV" 发明人 MURSKIJ GEORGIJ LEONIDOVICH;FAKEEV ALEKSANDR ANDREEVICH;POLISHCHUK OL'GA MIKHAJLOVNA;VENDILO ANDREJ GRIGOR'EVICH
分类号 C01D13/00;C07C51/41;C07C51/43;C07C53/10 主分类号 C01D13/00
代理机构 代理人
主权项
地址