摘要 |
<p>The present invention relates to the method for separating toluene diisocyanate from the post-reaction mixture in the toluene diamine phosgenation process in the gas phase. More specifically the solution concerns obtaining a higher TDI concentration in the liquid reaction product. The method is based on the fact that cooling and condensation of the reaction product - toluene diisocyanate - (TDI) is carried out by the application of spraying in the cooling and condensation zone, directly after the reactor, wherein this operation is carried out at a temperature elevated enough to obtain a low concentration of the solvent, i.e. within 5-30% by weight, in relation to TDI obtained, and thus a high concentration of (within 70-95% by weight) TDI obtained.</p> |
申请人 |
ZAKLADY CHEMICZNE ZACHEM S.A.;POLITECHNIKA WARSZAWSKA;INSTYTUT CHEMII PRZEMYSLOWEJ IM. PROF. IGNACEGO MOSCICKIEGO |
发明人 |
BALDYGA, JERZY;HENCZKA, MAREK;SZARLIK, STEFAN;ILMURZYNSKA, JANINA;DYCZEWSKI, MICHAL;SLAWATYCKI, ARKADIUSZ;CHRUPALA, WOJCIECH;LACHMAJER, JERZY;RUCZYNSKI, LECH;WOJCIK, LUCJAN;STUCZYNSKI, JACEK |