发明名称 |
USE OF AN ACETIC ACID WASH TO PREPARE LOW-SULFATE 5-SULFOISOPHTHALIC ACID, MONO-LITHIUM SALT |
摘要 |
There is disclosed a process for making a mono-lithium salt of 5-sulfoisophthalic acid (LiSIPA) having less than 500 ppm sulfate. The process uses a reaction mixture of water, a lithium cation producing compound, and 5-sulfoisophthalic acid. The reaction mixture is heated to reflux, cooled, filtered and washed with acetic acid to obtain a high quality LiSIPA having less than 500 ppm sulfate. Also disclosed is a high quality, non-purified reaction product containing a mono-lithium salt of 5-sulfoisophthalic acid and having less than 500 ppm sulfate.
|
申请公布号 |
CA2815049(A1) |
申请公布日期 |
2012.04.26 |
申请号 |
CA20112815049 |
申请日期 |
2011.03.29 |
申请人 |
FUTURE FUEL CHEMICAL COMPANY |
发明人 |
OSTER, TIMOTHY A.;COLEMAN, MICHAEL TODD |
分类号 |
C07C303/32;C07C303/44;C07C309/58 |
主分类号 |
C07C303/32 |
代理机构 |
|
代理人 |
|
主权项 |
|
地址 |
|