发明名称 BNA CRYSTAL
摘要 <P>PROBLEM TO BE SOLVED: To provide a method for producing a high-quality BNA (N-benzyl-2-methyl-4-nitroaniline) crystal. <P>SOLUTION: The method for producing the BNA crystal uses a solution method including a process of obtaining a seed crystal and a crystal growth process of growing the obtained seed crystal in a solution. In the crystal growth process, the seed crystal is retained by a crystal retentive member at the end of the seed crystal in the main growth direction. The solution used in the crystal growth process is a supernatant solution obtained after depositing the seed crystal in a process of obtaining the seed crystal. In a rocking curve measurement by an X-ray diffraction method, the obtained BNA crystal has a half width of diffraction-peak X-ray intensity being 100 second or lower. <P>COPYRIGHT: (C)2012,JPO&INPIT
申请公布号 JP2012012236(A) 申请公布日期 2012.01.19
申请号 JP20100148073 申请日期 2010.06.29
申请人 INSTITUTE OF PHYSICAL & CHEMICAL RESEARCH 发明人 SAITO MIKIKO;NOTAKE TAKASHI;MINAMIDE YASUTSUGU;ITO HIROMASA
分类号 C30B29/54;C30B7/08 主分类号 C30B29/54
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